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To ensure that the foam tip had fully expanded, measurements were taken two min after insertion for both the brass-cavity and ear-canal measurements.
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The measured data were processed using a mathematical statistics and subsequently, the expanded measurement uncertainty and confidence interval was calculated.
Multiplication of u c by 2 gave a resulting expanded measurement uncertainty of 13.2 %.
A reporting limit of 1.5 μg/L perchlorate and an expanded measurement uncertainty of 13.2 % were achieved.
The processed results with the expanded measurement uncertainty represent the B like reliable values at the next measurements with SCS.
We achieved a reporting limit (RL) of 1.5 μg/L perchlorate and an expanded measurement uncertainty calculated according to ISO 11352 [2] of 13.2%.
Even after allowing for an expanded measurement inaccuracy of 50%, the concentration of pesticide residues exceeded the prevailing limits in 281 of the samples.
The expanded measurement uncertainty (k = 2) of the temperature obtained by the pyrometry method was ±4 °C, for temperatures between 700 and 850 °C.
The indication of quantitative results from standard calibration experiments below the reporting limit of 1.5 µg/L (samples 3, 6, 16, and 17) needs to be specified including the expanded measurement uncertainty.
Participants were asked to perform two or three independent measurements, correct their measurements for recovery and for the moisture content, and report their calculated mean (expressed as mg kg−1 in dry mass) and its associated expanded measurement uncertainty (U lab).
These two results deriving from two independent traceability chains and via qNMR measurements of different nuclei are fully consistent and overlap within their expanded measurement uncertainties, as shown in Fig. 5.
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CEO of Professional Science Editing for Scientists @ prosciediting.com