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But as land in Manhattan between 14th and 96th Streets was extremely valuable even then, it was designated an excluded zone.
Only three of these residues (V36, R39, and D66) are within the 13 Å excluded zone.
The average Rex for these residues is 2.1 rad s 1 (2.0 rad s 1 for those outside the 13 Å excluded zone), with a range of 0.2 7.5 rad s 1 (0.2 6.0 rad s 1 for those outside the 13 Å excluded zone).
There are 24 model 4 residues for the 0.8 mM data at pH 6.5 (19 outside the 13 Å excluded zone).
A set of 23 residues were best fit by model 4 (20 outside the 13 Å excluded zone), which requires S, Rex, and τe (=τf).
For the 0.8 mM data at pH 6.5, there are 19 residues that show model 3 behavior (nine outside the 13 Å excluded zone).
For NP4 sym) at pH 7.3, the average S value was found to be 0.83 ± 0.04 (0.82 ± 0.03 for those outside the 13 Å excluded zone).
Four residues were best fit to model 5 (two outside the 13 Å excluded zone), which requires S, Sf, and τe (=τs).
At pH 7.3, the program found best fits for 73 residues (70 outside the 13 Å excluded zone) as model 1, meaning R2eff values are not dependent on the CPMG field for those residues, while at pH 6.5, the number of residues found to be model 1 decreases to 77 (67 outside the 13 Å excluded zone).
At pH 7.3, the program found best fits for 17 residues as model 2 (15 outside the 13 Å excluded zone), while at pH 6.5, that number increased to 28 (22 outside the 13 Å excluded zone), meaning in both cases that kex and Rex could be calculated.
Two residues (both outside the 13 Å excluded zone) were best fit by model 2, which requires τe (= τf = 100 200 ps) in addition to S. Another set of 91 residues (64 outside the 13 Å excluded zone) were best fit by model 3, which requires S and Rex.
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com