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The synthesis of amide 172 was also achieved by treatment of tosylate 171 with an excess of aqueous methylamine and followed by amidation with acid 65.
When polarized, an electrode surface accumulates charge and electrostatically retains an excess of aqueous cations or anions (the point of zero charge of a Hg electrode is around −0.5 V vs. Ag/AgCl [25, 26]).
The excess solvent was evaporated by continuous stirring for 45 min to 1 h followed by centrifugation at 10,500 rpm for 15 min to remove excess of aqueous solution.
The amount of genomic DNA was reduced to a minimum in order to maintain an excess of aqueous droplets over template molecules.
The DOTA modified heterostructures were then conjugated with Gd3+ by mixing solution of NPs with a large excess of aqueous solution of GdCl3.
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After electrophoresis, this small gel area was excised from the gel slab, and the proteins were fixed in the gel slice with an excess volume of aqueous solution containing 40% methanol and 10% acetic acid.
The aqueous Fe(II) concentration (ca. 400 1000 μM) was always in excess of the aqueous S -II) concentration (from below detection to 15 μM; detection limit, 1.2 μM; Table S -IIupporting Information [SI]).
The final product (AHP) was obtained by treating 40z with excess of 50% aqueous hydroxylamine for 24 hours [31].
The concept of hydration is used for evolving a new representation for the excess free energy of aqueous single-electrolyte solutions.
The concept of ionic hydration has been used earlier to get a new representation of the excess free energy of aqueous, single-electrolyte solutions, which leads to the prediction of γ± and φ values using only two parameters for each electrolyte at 25°C.
ZnS nanocrystals contain excess of sulfur in aqueous micellar solution, and thus show weak emission due to sulfur vacancies, but the emission became intense when excess of sulfur has been removed from the redispersed sample.
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