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However, the samples must be taken to the instrument for ex situ analysis.
Ex situ analysis using optical microscopy (OM) and surface roughness measurements provides an insight as to the events leading to the changes in surface texture observed in LLS.
Furthermore, ex situ analysis of the SEI requires separation and isolation of the SEI, which may change the content and the structure of the SEI.
This might be due to the exothermic oxidation reaction of deposited carbon compounds, characterized by ex situ analysis, with oxygen supplied by the sulphated support.
Atomic Force Microscopy (AFM) for ex situ analysis of the nucleated islands has been performed using a Veeco Innova microscope operated in tapping mode with ultra-sharp tips (nominal tip radius about 2 nm).
From the ex situ analysis of the spent catalyst samples the most probable mechanism of the high temperature sulfuric acid decomposition reaction was also proposed, which involves metal sulfate formation and decomposition steps.
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Through such ex-situ analysis, it could be possible to have prior knowledge, quantification and differentiation of the potential of chars manufactured from various feedstocks.
Ex-situ analysis validated that plating occurs only for the cells aged at −10∘C, but not for the cells aged at 25∘C.
On-line measurement by OES (Optical Emission Spectroscopy), ex-situ analysis by LIBS (Laser Induced Breakdown Spectroscopy) and ICP techniques demonstrated that elimination of metallic impurities and boron depends on the applied bias, and/or on the plasma gas composition.
The ex-situ analysis of strain, crack formation, dislocation density, and microstructure of the SL layers has established that the mechanism of strain relaxation in these structures depends on the residual strain in substrate and is determined mainly by the lattice mismatch between layers.
Multigrain XRD provides accurate unit cell determination for individual phases in a multiphase system and may serve as an in situ probe for the spatial distribution of compositional changes and/or chemical variation within a sample region of interest, complementing ex situ chemical analysis by TEM or other analysis techniques.
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