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But what was clicking in the first half -- when they led by as many as 11 points -- started to evaporate down the stretch.
W. VIRGINIA 62, GEORGETOWN 58 Johannes Herber tied a career high with 15 points and West Virginia nearly let a 13-point lead evaporate down the stretch before holding on at home.
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The fraction from 24 to 36 min was collected (36 mL) in a round flask and evaporated down to approximately 1 mL by means of a rotary evaporator (40 °C, 750 mbar).
The mixture was gently heated on a hot plate after adding few boiling chips, and evaporated down to about 20 mL.
When the evolution of H2 had ceased, sulfamoyl chloride (∼0.69 m in toluene,[ 19] ∼3–5 equiv, evaporated down to ∼1 mL prior to addition) was introduced in one portion.
The mixture was then centrifuged and the supernatant evaporated down to the aqueous residue, which was partitioned between acetate buffer (0.1 M, pH 4.5) and diethylether.
The resultant supernatant was pooled with the first sample and evaporated down to the aqueous residue, to which methanol (70% in water) was added and left overnight at –20°C.
To a solution of 24 a (300 mg; 1.31 mmol) and 2,6-di tert-butyl-4-methylpyridine (270 mg, 1.31 mmol) in anhydrous DMF (20 mL) at 0 °C under N2 was added sulfamoyl chloride (∼0.69 m in toluene,[ 19] ∼3–5 equiv, evaporated down to ∼1 mL prior to addition).
But more importantly, since it has evaporated down the U.S. media's "memory hole," Almagro was part of a vigorous international campaign to de-legitmize the congressional elections in Venezuela last December.
The media (1 mL) was treated with an equal volume of cold acetone to precipitate the protein and the solution was then evaporated down to <0.5 mL to drive off the acetone.
Evaporated, and rained down, and evaporated, and rained down.
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