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But insisting on them prior to entry amounts to "misplaced paternalism", according to Mr Buiter.
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Table 3 Evaluation of catalytic activity of DBSNa in the synthesis of (5a) a Entry Amount of DBSNa (mol %) Time (min) Yield b 15906821070810 70 81 3 15 60 87 4 20 60 94 5 25 60 94 a The reaction was carried out with 1-thia-4-azaspiro[4.5]decan-3-one (3) (10 mmol), benzaldehydes (4a) (10 mmol) and DBSNa in 10 mL acetic acid at room temperature.
Table 1 Optimization of the reaction conditions Entry Amount of catalyst (mg) Solvent Time (min) Yield 1 20 - 60 60a 2 20 THF 60 70 3 20 MeCN 60 81 4 20 EtOH 60 93 5 20 EtOAc 60 75 6 20 Toluene 60 85 7 18 EtOH 30 94 8 15 EtOH 10 95 9 10 EtOH 10 95100 5 EtOH 20 90 All reactions carried out at room temperature.
He leafed through it, increasingly shocked: the entries amounted to a journal of terror.
This knee-slapper comes from "Philogelos," or "Laughter-Lover," a Greek joke book, probably compiled in the fourth or fifth century A.D. Its 264 entries amount to an index of classical humor, with can't-miss material on such figures of fun as the miser, the drunk, the sex-starved woman and the man with bad breath.
The book consists of 7,471 volumes of entries amounting to 5,244,111 pages of text, plus a 36-volume index of the almost 7.5 million named contributors.
Prior to this study, organelle DNA sequence data for D. salina was limited to 14 GenBank entries amounting to 6.7 kb of ptDNA, divided over six protein-coding loci (no mtDNA sequence data were available).
With about three million entries, it amounts to the largest office pool in the world.
However, investigators reported finding handwritten ledgers with coded entries for amounts from $13,600 to $2 million stashed in offshore bank accounts.
There has been concern among Championship clubs that the entry criteria amount to a restraint of trade given the myriad demands that need to be met.
The anti-EU brigade is convinced that Mr Cameron will find it hard to "do a Wilson -- the Labour Prime Minister Harold Wilson, who won an In vote in the 1975 referendum after claiming that a tiny tweak to Britain's EU entry terms amounted to a renegotiation.
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