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Be careful with heating.
Liquid chromatography (Waters e2695 Separation Module) together with heated electrospray ionization mass spectrometry (Thermo Finnigan TSQ Quantum) was used to detect the intermediate products of sulfonamides degradation.
Help with heating bills.
Detection and quantification of analytes was achieved with a Thermo TSQ Quantum Ultra triple quadrupole mass spectrometer via heated electrospray ionization in positive ionization mode.
MS conditions were as follows: full scan mode was employed for analysis of sulfadiazine, sulfamerazine, sulfamethoxazole, and their products; MS spectrometry ionization source was heating type electrospray ionization source (H-ESI), with specific parameters shown in Table 2.
For mass spectrometric analyses, the following parameters were used: positive ion mode, electrospray voltage: 4.5 kV, heated capillary temperature: 220°C.
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