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A 0.05 M Na2SO4 solution was passed through the electrode compartments.
Electrical power is harnessed by placing a load between the two electrode compartments (Allen and Bennetto 1993) (Fig. 2).
Thorough characterization of the products collected from both electrode compartments confirmed the production of ultrathin GNs (<5 layers).
Sections I and VII are the electrode compartments; II, IV, and VI are the concentration compartments; III and V are the desalination compartments.
In the current sensor design, both electrodes are exposed to the same test gas eliminating the need for isolating the electrode compartments.
During the remediation the suspension was acidified from water splitting at the anion exchange membrane and the acidification mobilized Cd that was removed to the electrode compartments.
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In addition, the Ag/AgCl reference electrode was connected to the working electrode compartment by a salt bridge.
A silver/silver chloride reference electrode was separated from the working electrode compartment by a salt bridge.
0.1 M Na2SO4 was used as electrode rinse solution circulating in electrode compartment, to prevent the generation of chlorine or hypochlorite, which could be hazardous for the electrodes.
The method employs a 'Swagelok' cell design equipped with a glassy carbon working electrode, in which redox species are placed initially in the counter electrode compartment only.
The design is inspired by PEM electrolysis technology and modified appropriately to allow light irradiation and to host a third electrode compartment, which enables the use of a hydrogen reference electrode.
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