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The effects of each aging method on the physical characteristics, rheological property and chemical composition of the binders were studied.
XPS and EDX characterization at each aging step enables a monitoring of the change in chemical composition during degradation.
The endothermic aging peak, relaxation enthalpy and fictive temperature were also calculated for each aging temperature and aging time.
Equilibrium Ni content at each aging temperature proved to be a crucial parameter in controlling the alloy properties, even in heterogeneous precipitations.
A total of 2834 test sections were used for E* predictions at ten temperatures amounting to a total of 28,340 data points for each aging condition.
Aging provided a significant rise in transformation temperatures (TTs) until they reached their equilibrium states, corresponding to the equilibrium Ni content at each aging temperature.
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