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Differential scanning calorimetry (DSC) analysis was done with Mettler DSC 822e (Mettler Toledo, Greifensee, Switzerland).
The polymorphs were examined by the IR and DSC analysis.
This fact was confirmed by differential scanning calorimetry (DSC) analysis.
Smaller or no endotherms were exhibited in DSC analysis.
In order to get more information about the chemical and structural nature of the spinae we performed differential scanning calorimetry (DSC) analysis.
These results were further confirmed by DSC analysis.
The crystallinity of the polymers was studied by DSC analysis.
The melting and crystallisation behaviour could be understood from DSC analysis.
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Same conditions were used for the cyclic isothermal P-DSC analysis.
P-DSC analysis from 1 bar to 1,000 bar were performed in a Setaram μDSC7 EVO equipment.
Pressure dependence of the transition temperature values (Tt) obtained from the onset temperatures of P-DSC analysis carried out under pressures from 1 to 1,000 bar both on heating (orange) and cooling (blue).
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