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He had brought over from Edgewood powdered LSD, which he would use to dust a drinking glass — leaving upon it "an imperceptible dry residue".
The evaporated dry residue was dissolved in 0.5 mL ethanol.
The sludge should be characterized based on % organic dry residue referred to the ignition loss of the dry residue.
The dry residue was resuspended in 1 mL of ultra-pure water.
After evaporation, the dry residue was dissolved in 50 μL methanol.
All samples (dry residue) were dissolved in 10% sterile dimethyl sulfoxide.
The dry residue (target value 2.5% ± 0.5%) and the ignition loss must be documented.
First, the dry residue was suspended with water (10 mL) and extracted with acetoacetate (10 mL).
The light petroleum extract was evaporated in vacuo to dryness to give 4.3 g dry residue.
The concentration of the extract was 100 mg/ml in relation to the dry residue.
High performance liquid chromatography revealed less than 0.13% monomeric sugars in the dry residue.
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