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The yellow solid was filtered, dried under suction and washed with ether (20 mL) to give the title compound as a yellow solid (6.57 g, 74%%).
Similar(59)
The solid was collected on a medium glass frit via suction filtration, washed with ethyl acetate (2 × 20 mL), and dried under vacuum (1 mm Hg) at 50 °C for 12 h.
Dry-Phrase The yellow product was dried under vacuum.
Panicles were air dried under natural conditions.
The extract was dried under reduced pressure.
Slides were dried under gentle nitrogen flux.
They were dried under vacuum.
Samples were then completely dried under vacuum.
Supernatants were dried under heated nitrogen (40°C).
The leaves were dried under shade.
The fractions were dried under reduced pressure.
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