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The aim of this study was to establish a double-correlation between the influence of the bilayer period and the deposition temperature on the resulting mechanical tribological properties.
H double quantum correlation spectra as well as REDOR-based heteronuclear (H−C) correlation spectra were recorded at 50 kHz MAS and 700 MHz H Larmor frequency on a Bruker Avance spectrometer using a Bruker 1.3 mm double resonance MAS probe with 140 kHz RF nutation frequency (1.8 μs 90° pulse length).
Other less prominent signals for resinol substructures (C) were also observed in the spectrum, with their Cα Hα, Cβ Hβ and the double Cγ Hγ correlations (Cα, Cβ and Cγ).
It is possible that the effect is the result of "holes" arising from destructive interference of the double quantum 14Nτ correlation frequency and 13C correlation frequency, with each possessing a different phase [49].
In general, the pairwise correlations of MZ twins were double compared to correlation of DZ twins suggesting genetic influences on sedentary behaviour (Table 3).
The corrections doubled the correlations to approximately 0.5.
To aid unknown metabolite identification, homonuclear two-dimensional (2D) experiments, such as H H double quantum filtered correlation spectroscopy (DQF-COSY) and H H total correlation spectroscopy (TOCSY) experiments, were performed on serum samples after protein precipitation using methanol (2 1 v/v).
Homonuclear two-dimensional (2D) experiments such as H H double quantum filtered correlation spectroscopy (DQF-COSY) and H H total correlation spectroscopy (TOCSY) experiments were performed for both ultrafiltered and protein precipitated serum samples using methanol to aid in peak assignment.
Double arrows indicate correlation between pairs of independent variables.
For example, if the ratio is 0.5 the effect of correction is to double the sample correlation.
Data from double arrows represent correlations between the variables whereas data from single arrows represent standardized regression weights (parameter estimates).
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