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The ethanol content in the substrates after SSF was measured before AD to demonstrate that most of the ethanol was distilled off during the distillation step.
The excess of solvent was distilled off at low temperature in a rotary evaporator.
About 40 mL of toluene was distilled off using a water separator.
Organic solvent was distilled off and the residue was fractionally distilled.
After refluxing for another 4 h, the solvent was then distilled off under reduced pressure, and the residue was PAA.
The solvent was distilled off and the residue obtained was washed with water, dried and recrystallized with hexane.
Similar(36)
Transferring the imine 22 a to a short-path distillation (Kugelrohr) apparatus in chloroform, distilling off the chloroform so that the neat sample could then be heated to 100 °C for 1 h gave complete conversion from the imine 22 a.
He obtained a yellow solution (probably cis [Os(OH 2O4]2−) before distilling off volatile osmium tetroxide, OsO4.
After each run the product was isolated by distilling off the solvent ether.
Compared with a traditional reflux system that maintains the ratio of water to ethylene glycol (EG) at ∼160 °C for ∼4 h, the gradual concentration increase of EG in the precursor solution can be accomplished by distilling off water in the OLRS while increasing the temperature to 130 °C.
But nothing, they say, is more authentic than freshly distilled mescal off the ranch.
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