The obtained results are in good agreement with results from similar manual techniques, while the whole determination process is also much faster than other automated electron backscattering diffraction analytical methods.
X-ray diffraction, analytical electron microscopy, differential thermal analysis and Fourier transform infrared spectroscopy were used to characterize the phase composition, elementary distribution, and microstructure in the feedstock and in the coatings.
Chemical composition and phases of HCWA were evaluated using X-ray Fluorescence (XRF) and X-ray Diffraction (XRD) analytical methods respectively.
The microstructure of titanium alloys (Ti 1Al 1Mn, Ti 6Al 4V) nitrided under glow discharge was characterised using light microscopy, X-ray diffraction and analytical electron microscopy.
Convergent-beam electron diffraction and analytical electron microscopy, especially the application of energy-dispersive X-ray and electron energy-loss spectrometry, have provided structural and chemical information in addition to strain contrast from lattice defects.
Analytical methods include X-ray diffraction (XRD), transmission-analytical electron microscopy (TEM-AEM), inductively coupled plasma optical emission and mass spectrometry (ICP-OES, ICP-MS), ammonium acetate extraction (1 M NH4OAc, pH = 7, for CEC) and C N analysis.
The crystalline phases of the materials were investigated using X-ray powder diffraction (XRD) PAN analytical X-ray diffractometer using CuKα radiation (λ =1.5406 nm).
They were characterized by FT-IR, UV Vis, mass, 1H NMR, ESR spectral studies, TG DTG, X-ray powder diffraction and physical analytical studies.
Based on the diffraction theory, the analytical solution of the wave pressure and the wave force on the composite bucket foundation is accurately derived by assigning reasonable boundary conditions.
Mixed ligand complexes were synthesised using nicotinamide as the primary ligand and nitrite as the secondary ligand were characterised by FT-IR, UV Vis, 1H NMR, TG DTA DTG, X-ray powder diffraction and physical analytical studies.
We investigate the structural changes of spinel lithium titanate (LTO; Li4Ti5O12) via the electrochemical Na insertion-extraction cycles, using X-ray diffraction (XRD) and analytical transmission electron microscopy (A-TEM).
