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The different dependences of hardness upon indentation depth in this work reveals clearly the local interaction between dislocations and grain boundaries in single grains.
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The different dependences of both the hardness and Young's modulus on loading rate and holding time were associated with creep deformation occurring during indentation testing.
The temperature dependence of hardness has been measured and, from the disappearance of indentation cracks and the measured energy density at different temperatures, the indentation brittle-to-ductile transition temperature TIBDT has been determined.
This showed that there was great dependence of hardness on calcium, magnesium, chloride and sulfate.
Figure 4 shows the dependence of hardness for two films on Si content.
In addition, the dependence of hardness on Si content should not have related to crystallization degree.
The result showed that there was great dependence of hardness on calcium, TDS, and alkalinity.
This result implies that there was great dependence of hardness on calcium, magnesium, chloride, sulfate, and bicarbonate.
The dependence of hardness vs. grain size had been previously calculated for titanium nitride and revealed that the maximal hardness (around 32 GPa) can be achieved for the material with grain size ~10 nm.
There is also little orientational dependence of hardness in spite of relatively large variations in ERSS (compared to the (010) face for example).
Besides, the glass transition temperature Tg of hybrids was determined from temperature dependence of hardness.
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