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First, the true and observed count rates, for each of the six energy windows, were determined (method B).
The determined method performance parameters include apparent recovery, matrix effects and extraction recovery.
Four different models were tested using TASSEL v.3.0 [ 64] to detect the most conservative one, using the P3D (Population Parameters Previously Determined) method and an optimum level of compression as estimation variables.
We determined method reporting limits (MRL) for each PAH on a batch-by-batch basis according to the contamination measured in the method blank (i.e., MRL = 3 × mass of PAH in the method blank).
The determined method also was to be Occupation Health and Safety safe, adhere to infection control standards and minimises risks of patient handling.
The further details of determined method were not described here.
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The three experimentally determined methods have identified 654 [ 18], 774 [ 16] and 688 [ 19] EGs.
Aliquots of these solutions were diluted and analyzed to determine method linearity.
Ethanol appeared to have no effect on the reducing sugar determining method.
We plotted precision-coverage curves, which are the standard for determining method performance.
They need to work at developing trust and determining methods for hashing out differences remotely.
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