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A specific characterization protocol was set up, entailing hot-stage microscopy and determination of phase composition and microstructure.
Determination of phase composition, structure and particle size are very important for the discussions on the physical properties.
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For determination of the influence of phase composition and surface morphology of obtained coatings on changes of corrosion resistance, these coatings were modified in argon atmosphere by thermal treatment at the temperature of 1100 °C during 1 h.
These experiments established the temperature range for which the largest differences are observed in molecular mobility in crystalline phase, semi-rigid crystal amorphous interface, and soft fraction of the amorphous phase allowing accurate determination of the phase composition and the thickness of these domains.
This technique enabled also the determination of quantitative phase composition.
microscopic determination of the phase composition is larger for the blend system under investigation.
The prepared samples were investigated through X-ray diffraction (XRD) and Scanning electron microscope (SEM) for the determination of their phase, composition and microstructural properties.
The determination of gas phase composition above the liquid oil has preliminarily required controlled temperature and pre-established equilibrium conditions.
Calculation of phase compositions from volumetric behavior for multicomponent mixtures.
The measurements of volume changes of cementitious materials thus produced, followed by the compressive strength tests, rate of hydration determination, phase composition studies and microstructure of hydration products observations have been carried out to find the optimum proportions of blended cementitious material, as the controlled expansion and hardening are concerned.
Investigation on a surface structure of iron modified by the action of compression plasma flows and determination of element and phase composition was carried out using X-ray diffraction analysis, Auger-electron spectroscopy, optical microscopy and scanning electron microscopy, along with studies on mechanical properties of the material.
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