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Monosaccharides were detected using a gold pulsed amperometric detector set on waveform A, according to the manufacturer's instructions.
Furfural and hydroxymethylfurfural (HMF) in pretreatment liquid samples were analysed with an HPLC system (Waters, Milford, MA, USA) equipped with a Biosil C18 column (Bio-Rad) and detected using a UV detector (Waters 2487 dual absorbance detector) set on a wavelength of 220 nm and operating at room temperature.
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HPLC was carried out on an Agilent (Santa Clara, CA) 1100 LC system equipped with variable wavelength absorbance detector set for monitoring pNP and MU derivatives (310 nm).
Glucose, ethanol, glycerol, acetate, succinate, citrate, fumarate, malate, oxalate were detected on a Waters 410 differential refractometer detector (Shodex, Kawasaki, Japan), and acetate and pyruvate were detected on a Waters 468 absorbance detector set at 210 nm.
Phloroglucinol adducts were determined on the basis of chromatograms registered with the PDA detector set at 280-nm wavelength.
Homogeneity of the isolated fractions was analyzed by reversed-phase HPLC on a Waters HPLC 2690 Module and a Waters UV 2487 detector (set at 288 nm).
The source was placed at the origin, the boxes were placed with their centres at 50 cm intervals along the x axis, whilst the detector was set on the x = 0 plane.
The diode-array detector set at 360 nm.
The accompanying apparatus, which has already been tried out on a small, intact reactor, consists of two billboard-size detectors, set up on opposite sides of the building.
Furthermore, she found that one of the motion detectors they'd set on the deck had been knocked over.
A full diffraction pattern was collected as a function of energy simultaneously on three detectors set at 2θ angles of 2.92°, 5.44°, and 8.32°.
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