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Its entrance is now blocked by a metal detector; armed cops share the corridors with teenage girls.
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The horizontal syringe was taped to the imaging table with the plunger head pointing towards the vertical detector arm.
The vertical syringe's plunger required pruning to avoid collision with the upper CZT detector arms as the syringe is filled with water.
The end-station will allow measurements of solid samples, solutions and interfaces in a wide range of experimental conditions with high energy resolution covering a large Q-range realized by a continuous rotation of the RIXS detector arm by 120°.
Because of the high X-ray energy, the beam attenuation is negligible and by an appropriate positioning of the detector arm slits it is possible to minimize the diffuse scattering induced by the liquid and cell walls in order to still detect the minima of the crystal truncation rods (CTRs).
The hardware of the detector arm with mounted spectrometer is shown in Fig. 2 as well as the mounted detector arm in the ultracentrifuge.
The entire setup of the second-generation detector arm is still modular it can fit into every preparative and analytical Beckman ultracentrifuge.
The second method reduced the time taken recording a map by rocking the analyser crystal rather than moving the detector arm, as very small analyser rotations,, approximate to detector movements,.
The remaining 90% of the light is sent toward the reference arm where it is back reflected by the mirror and passed to the detector arm where it interferes with the light back scattered from the sample.
We have improved the design in the second-generation detector in a way that the UV/Vis spectrometer entrance slit (Ocean Optics, USB 2000) is now mounted on top of the detector arm at the focal position of the colliminating lens where the light was coupled into the fiber again in the first-generation design.
This requires that neither the sample nor detector arm include linear polarizers, and that the Jones vector of the light returning from the reference arm have nonzero components along both axes of detection (e.g., E r must not be horizontally or vertically polarized).
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com