This deduction was confirmed by the COSY correlation of H-6″/H-7″ and the HMBC correlations of H-6″/C-8″; Me-9″/C-7″, C-10″; and Me-10″/C-7″ (Fig. 2).
The above deduction was confirmed by the MS2 experiment on 2a, which gave rise to the expected ions 2b (m/z 341) and 2c (m/z 297), and the subsequent MS3 experiment on 2b in which the fragment ion at m/z 297 (2c) was further detected.
Relegation was confirmed for Hearts last month, with a 15-point deduction for being in administration at the start of campaign a major factor in their demotion.
PSG's title will not, however, be confirmed until a league disciplinary panel meets to decide whether to impose a points deduction following allegations that their sporting director, Leonardo, barged a referee.
The Poppies have recently had a company voluntary arrangement approved by creditors, and have been confirmed a place in the Southern Premier for 2012/13, albeit with a ten-point deduction.
QPR have been confirmed as npower Championship title-winners after the Football Association revealed they will face a £875,000 fine instead of a points deduction.
This deduction was also confirmed by the MS3 analysis from the parent ion 4B.
This deduction was further confirmed by an X-ray diffraction experiment using Mo Kα radiation (Fig. 4).
This deduction was further confirmed by the HMBC correlations of NH (δ H 6.35, s) with C-20, C-21, C-22, and C-23, of H-23 with C-20, C-21, C-22, and C-17, together with the 1H-1H correlationstiofs of NH/H-23/H-22 NH/H-23/H-22 NH/H-23/H-22
And the penalty is generally that the deduction is disallowed.
