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The thermal stability measurement of the chemically modified GDLs showed rapid decrease of sample mass during heating.
The steep decrease of sample mass between 500 and 600 °C is related to PTFE decomposition [31, 32].
From (28), (29) we can see why the estimate variation is increase as the decrease of sample points.
The moisture content was evaluated by the decrease of sample weight at the end of an isotherm at 120 °C.
Therefore, we excluded these samples from analysis, resulting in a decrease of sample size to 26 PD (14 males and 12 females) and 21 non-PD samples (10 males and 11 females).
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With the decreasing of sample amount for training model, the Cubic SVM classifier still performs well in classification with accuracy of 86.9%.
On one hand, the decreasing of sample points is desirable for signal processing.
On the contrary, decrease of the sample cooling rate drastically changes the structure of the surface.
In all cases, the decrease of the sample mass after laser illumination was observed.
From left to right, the number of positive signals (green) decreased obviously with the decrease of the sample concentration.
The weakening and broadening of the XRD peaks may be attributed to the decrease of the sample grain size and the increase of the SiO2 content.
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