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The characteristics of the internal curing material used to improve the performance of heat-cured concrete should be consistent with the heat-curing regime and match those of the cement paste.
It also resulted in a better interfacial transition zone with a more homogeneous distribution as well as a microstructure with a lower porosity around the internal curing material (lightweight fine aggregate) in the case of the heat-cured mortar.
In an immersed not yet fully cured material, the continuation of curing and plasticization concurred.
Thus, dicumyl peroxide had to be used to obtain the cured material and avoid degradation.
The harder MBOCA cured material did not show slow crack growth and failed rapidly.
Amorphous character of the cured material is determined using X-ray spectroscopy.
The MBOCA cured material of lower hardness also showed slow crack growth, but crack growth started at much higher strain energy densities than for the Ethacure E300 materials.
Both approached the values of those of the fully cured material; the E-modulus after one month and strength after 20 months.
These reactions, that occur in solution at room temperature, can significantly reduce the glass transition temperature of the fully cured material.
The morphology of the final, cured material was probed by wide-angle X-ray scattering, as well as optical and atomic force microscopy.
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