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The crude solid product was filtered off and recrystallized from DMF, yield 85%, mp.
The crude solid was filtered off and recrystallized from ethanol to give the corresponding hydrazides ZE-3(a c) [14].
The resulting crude solid was cooled to room temperature and refluxed in 25 mL of dry ethanol (EtOH) for 1 h and then cooled to room temperature.
The nanocrystalline MgO was filtered off and the reaction mixture was cooled to ambient temperature, and the crude solid residue was recrystallized from ethanol and water to afford pure crystals of the proper pyrido[2,3-d]pyrimidines in 84 96 % yields.
The crude solid was dissolved in EtOH (30 mL) followed by the addition of conc.
The resulting crude solid was recrystallized with methanol to yield corresponding amide.
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Open image in new window Fig. 3 Viscosity versus shear rate measured at 30 (diamond), 45 (circle), 60 (square) and 80 °C (triangle) of the crude oil (solid symbols) and emulsions (filled symbols) prepared with 70% oil content and 3 wt% Triton X-100 Open image in new window Fig. 4 Exponential Arrhenius-type association of crude oil with the temperature.
Comprehensive testing of waxy crude oil solid deposition using a recently developed device based on Taylor Couette flow under both live (single-phase) and stock tank conditions was performed.
Our six pioneers are kindred spirits to those who produced crude solid-state electronics after the invention of the transistor or who roughed out the Internet in the early 1970s.
The resultant red crude solids were dissolved in 250 mL of water with 0.1% TFA.
Pyrolysis is the heating of biomass in the absence of oxygen and results to liquid (termed bio-oil or bio-crude), solid, and gaseous fractions in varying yields depending on a range of parameters such as heating rate, temperature level, particle size, and retention time.
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