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Since our aim was to obtain high quality quantifiable data with minimal operator input and bias, we adopted a micropillar geometry for the cross sectional specimen preparation, rather than the conventional lamella geometry.
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These results have been tested by examination of cross sectional specimens by transmission electron microscopy (tem), prepared by ultramicrotomy techniques which showed that the barrier film was missing at some sites and significantly flawed in others.
The preparation procedures of the cross-sectional specimen for TEM observation are as follows.
A typical example of our images is shown in Fig. 1 for the cross-sectional specimen of 5, 15, and 30 nm film thickness, respectively.
Energy-filtered transmission electron microscopy [EFTEM] was carried out on a cross-sectional specimen using a TEM-FEG microscope Tecnai F20ST (FEI, Eindhoven, The Netherlands) equipped with an energy filter TRIDIEM from Gatan (Gatan, München, Germany).
Slate flexural strength was compared for two distinct situations: (i) using a 3-Point flexure loading configuration in batches of materials with larger cross-sectional specimen dimension (50 × 30 mm2); and (ii) using a 4-Point flexure loading configuration in the same batch of materials but with smaller cross-sectional dimensions (30 × 25 mm25.
High-resolution TEM imaging was performed from two cross-sectional specimens.
The formation and evolution of Ge-NCs have been investigated using high-resolution electron microscopy (HREM) on cross-sectional specimens.
Cross-sectional specimens suitable for HR-TEM were prepared using a focused ion beam (FIB) FEI Quanta FEG dual-beam system (FEI Co).
A second compression fixture was developed to axial load omega cross-sectional specimens with strain rates from 2×10−4 to 5s−1.
TEM observations were done in an FEG 2200FS JEOL instrument on <011> cross-sectional specimens prepared by the standard sandwich procedure and finally thinned with Ar ion bombardment.
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