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The resin was washed with DMF (2 × 5 mL) and then three times with a copious volume of CH2Cl2, filtered, and dried in a vacuum.
The resin was washed with DMF (3 × 3 mL) and then three times with a copious volume of CH2Cl2, filtered, and dried in vacuum.
Boc-aminooxy acetic acid (123 mg, 0.64 mmol, 12.0 equiv), HATU (237 mg, 0.64 mmol, 12.0 equiv) and 2,4,6-trimethylpyridine (110 μL, 0.83 mmol, 16.0 equiv) were added to the resin and the reaction mixture was agitated for 90 min. The resin was washed with DMF (3 × 3 mL) and then three times with a copious volume of CH2Cl2, filtered, and dried in vacuum.
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Neither, surely, has any British politician ever produced so many and such copious volumes of diaries - eight published to date.
Zn was reactive in ammonia-ammonium buffer and generated copious volumes of gas which increased with pH from 8.1 to 10.5.
They give the book to Astrid, a skilled decoder, along with copious volumes of data from biotechnology corporation Massive Dynamic about the numbers stations.
A related argument for a freshwater origin concerns the presence of a glomerular kidney and a distal tubule segment, the main functions of which are to produce copious volumes of hypo-osmotic urine to counteract the osmotic influx of water in the freshwater teleost [52], [53].
Copious volumes of liquid waste that might conceivably be generated by (for example) a large animal feeding study may need to be handled by a professional liquid waste disposal agency.
It has, however, kept his "Selected Poems" and several other collections of his writings in print at New Directions, which first published him in the thirties, and also resulted in the publication of a volume of his letters and a copious selection from his unpublished notebooks.
In her 1663 volume of Palladio's writings she wrote copious notes about building techniques and raw materials.
We suggested that humidity gradients are likely to occur in other long-tubed or -throated flowers with an interstitial volume of air within the flower bud and copious nectar production, all characteristics of the hawkmoth pollination syndrome.
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