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Analysis of deconvoluted C1s peak in XPS spectra confirmed surface chemical modification at each functionalization step.
Test results confirmed surface changes through plasma treatment, amine and antioxidant modification.
XPS and ICP confirmed surface composition while Brauner Emmett Teller (BET) analysis was used to define the specific surface area.
FTIR analysis in the range from 900 1200 cm− 1 and 2850 3000 cm− 1 confirmed surface modification and re-orientation of the attached molecules.
XPS analysis, topographic and phase imaging by atomic force microscopy (AFM) further confirmed surface modification by AuNPs and also their functionalization.
An initial evaluation found inconsistencies of treatment effect between blocks, and an as-built survey later confirmed surface elevations within Block 3 deviated from the intended design and was excluded from further analysis.
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Water contact angle, atomic force microscopy (AFM) and microscopy were used to characterize and confirm surface modifications, and the non-fouling performance of the resulting surfaces was tested using both live and dead CCRM-CEM cancer cells.
FTIR spectra for Br MSN exhibited peaks of both the N H bending vibration of APTES at 1617 cm–1 and C N stretching vibration of Bromelain at 1517 1587 confirmingrming surface functionalization of MSN.
To confirm surface-exposure of these proteins in transformed B. garinii, immunofluorescence microscopy was conducted using live bacteria and polyclonal antibodies specific for either CRASP-3 or CRASP-5 [40].
The methoxy film formation during cathodic polarization of the metal surface was confirmed by surface structure measurements.
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