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In these conditions the valuable compounds were from two to four times more concentrated than in classical hexane extraction.
Limits of detection for the selected target compounds were from 0.003 to 0.01 μg/L and 0.01 to 0.5 μg/L, in MS and MS/MS mode, respectively – by direct sample injection of 100 μL.
All chemical compounds were from Sigma Aldrich and dissolved directly into ND96 recording buffer to a final concentration of 10 mM unless otherwise noted.
BEL compounds were from Cayman Chemical.
All compounds were from Sigma-Aldrich.
Three-dimensional structures of compounds were from NCBI.
Similar(44)
495 compounds are from Li's dataset [33] and 66 from WOMBAT-PK [34] database; the other 245 compounds are collected by PKKB from publications.
The greatest source of exposure to these compounds is from farmed salmon (Salmo salar).
The chemical library containing 2000 biologically active compounds was from The Spectrum Collection (MicroSource Discovery System, Inc. Gaylordsville, CT 06755).
A library of 324 754 compounds was from NIH.
TRIM24-C34 compound was from Xcompound
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