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The main wear mechanism in the compound layer was microcracking.
The compound layer thickened slightly with increased frequency.
The thickness of the compound layer was about 400 μm.
The results showed that the compound layer had a deleterious effect.
The elemental depth profiles of the compound layer were investigated by glow discharge optical spectroscopy.
The nitrogen concentration and the compound layer thickness increase, when 10% of C2H2 is added.
The results show that the nitrided layer consists of a compound layer and diffusion zone.
A transition layer is present between compound layer and diffusion layer.
It was found that the compound layer consists of the dominant γ′-Fe4N phase.
For the highest nitrogen concentration and lowest bias voltage, no compound layer was formed.
These conditions prevented formation of an undesirable compound layer in the nitrided layer.
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