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Chemical composition of the specimens was analyzed using an EDS as attached on the SEM.
(ii) Despite the abundant cluster emission the In/P bulk composition of the specimens (i.e., away from any surfaces modified by ion bombardment) turns out to be correctly reproduced by APT, provided the laser pulse energy is 10 pJ or less.
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Therefore, the BE-SEM image reflects the distribution of chemical composition of the specimen.
Finally, chemical analysis of the recrystallized efflorescence provided an accurate assessment of the ionic composition of the specimen.
The elemental analysis was done by the energy-dispersive X-ray spectroscopy S-48000, Hitachi, Japan) to determine the relative composition of the specimen.
To relate a morphological structure of polymeric specimens to the applied conditions of the production process requires to be able to analyse the morphology and composition of the specimen with high spatial resolution, ideally with a single technique.
The determined Ge content in the initial section of the depth profile (0 6 nm) has an overestimated value, and it corresponds to the technological composition of the specimen buffer layer 10 at.% in the final section of the depth profile (7 10 nm).
Indeed, radiation damage is a complex phenomenon that remains under active investigation, since it depends not only on the chemical composition of the specimen but also on multiple data collection parameters such as cumulative dose, imaging temperature (Comolli and Downing 2005; Iancu et al. 2006; Bammes et al. 2010), and dose rate (Chen et al. 2008; Karuppasamy et al. 2011), among others.
This data represents the unaltered structural composition of the specimen, in contrast to classical histological or dissection techniques and apart from fixation.
Changes of the chemical composition of the test specimens during ageing of the treated test specimens are assumed to cause increased leachability of copper.
To confirm the presence of HA in the BC membrane, we performed XPS analyses of the surface elemental composition of the BC specimens.
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