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At the completion of the polymerization, the incorporated percentage of the lowest HLB emulsifier was 61%, much higher than that of the highest HLB one (10%).
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To ensure completion of polymerization within the coprecipitated nanoparticles, the mixtures were further stirred at room temperature for 20 h.
FT-IR spectrum implied that the characteristic absorption peaks of the benzoxazine ring disappeared completely after curing at 240 °C for 1 h, which illustrated that the completion of polymerization reaction.
One additional cycle at 72°C for 7 min was included after the last cycle to allow completion of incomplete polymerizations.
The time (t1 + t2) needed for completion of the first two stages is inversely related to the rate of polymerization.
This shows the progress of the polymerization reaction.
The duration of the polymerization was about 4 h.
Bifunctional monomers might improve the polymerization process by providing more reactive groups and the extent of the polymerization reaction [ 2].
If this comonomer (VBIC) affects the polymerization, where is it located at the end of the polymerization?
"This is the completion of the revolution".
Completion of the factory has been delayed.
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