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At the completion of the monitoring period, the electrodes were removed and the seizure focus was resected.
Upon completion of the monitoring period on the 65th day of operation, due to declining power production, the MFCs were disassembled.
The year 2015 marks the completion of the monitoring period for the Millennium Development Goals which will be replaced by the Sustainable Development Goals currently being negotiated by the international community.
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After completion of the reaction (monitored by TLC), the mixture was cooled to room temperature and the solvent was evaporated.
Following the completion of the reaction (monitored by TLC), it was quenched with the addition of ice cold water and extracted with ethyl acetate (3 × 25 mL).
Following completion of the reaction (monitored by TLC), the solvent was evaporated under reduced pressure to obtain a crude product which was purified by PTLC using hexane:EtOAc (75:25) as eluent.
After completion of the reaction, monitored by TLC, the solid product was filtered, washed with ether (3 × 20 mL) and dried to obtain pure products 4 and 5. 4a, as colorless crystal (1.5 g, 2.76 mmol, 92 %).
Upon completion of the reaction (monitored by TLC, 1 2 h), the products were purified by chromatography or crystallization.
The reaction mixture was stirred at room temperature for 10 min. After completion of the reaction (monitored by TLC), the reaction mixture was diluted with CH2Cl2 (20 mL), and the organic layer was then washed 2 times with 5 mL of saturated aqueous NaHCO3.
After completion of the five- day monitoring period, participants returned the accelerometer and completed the remaining questionnaire.
General procedure for the aza-Michael additions: To a flask containing an equimolar mixture (1.5 mmol) of amine 4 and chalcone derivative 3 in methanol (1.5 mL), 100 mg of catalyst (ABM, KF/ABM or NaNO3/ABM) was added and the mixture was stirred at room temperature until completion of the reaction (TLC monitoring).
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