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Upon completion of addition, the solution was stirred at reflux for 2 h.
After completion of addition of NaBH4, the ice bath was removed, and the reaction was allowed to proceed at RT for 16 h.
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Upon completion of the addition, an additional 0.25 mL of 5%% hexachloroplatinic acid solution was added and the mixture was stirred at 100 °C for 45 min. GC analysis of the mixture indicated the presence of some unreacted pentachlorodisilapropane.
Upon completion of the addition, the mixture was stirred at 25 °C for 15 h.
Upon completion of the addition, the temperature of the reaction mixture was allowed to warm to room temperature.
After completion of the addition, the reaction mixture was warmed up to room temperature for another 2 h, and was cooled again with ice bath.
Upon completion of the silane addition, an additional 0.25 mL of the catalyst solution was added and the reaction mixture heated at 95° for 45 min. Distillation provided 80 g (70%%) of the title organosilane.
After completion of the metal addition, the mixture was stirred for an additional 30 min.
After completion of the olefin addition, the reaction was heated for an additional 3 h at 130 °C.
Delmhorst & Sheehan characterize Stamford as the central business district of the region, arguably validated by the completion of UBS Warburg's addition to its American headquarters on Washington Boulevard.
Govan has overseen the completion of several major additions to the museum after the collapse of the Koolhaas plan — including two buildings on the west side of the LACMA campus by architect Renzo Piano, the Broad Contemporary Art Museum and the Resnick Pavilion.
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