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After reaction was completed, solvent was removed using a rotary evaporator.
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Once the previous simulations were completed, solvents containing CO2 were evaluated.
Once deesterification was completed, the solvent in RV2 was evaporated in vacuo, and the radioactivities of the solvent in the column, RV1, and RV2 were measured upon the completion of F-FPAMT.
After the addition was completed, the solvent was removed under reduced pressure and the crude purified by CC (silica; Et2O / n-hexane 1 2) to yield the title compound 8a (22 mg, 21%%): mp 81 82°C (Et2O / n-hexane).
10 gm of white oil was added as a diluent to faciliate stirring, and after the reaction was completed the solvent was removed using rotary evaporator and at 90 °C compounds (A1, A2) were obtained.
When the extraction was completed, the solvent microdrop containing the enriched analytes was retracted into the microsyringe and directly analyzed by GC MS without any filtration or cleanup step.
In fact, the bead formation prevention is attributed to the complete solvent evaporation at optimal distance.
Then, vinylated nanoparticles were dried at 110 °C until the complete solvent removal.
Therefore, the delay of curing might only help assure complete solvent evaporation before hardening.
The mixture was stored for 24 h at 37 °C to assure the complete solvent removal.
Complete solvent removal required heating under vacuum up to well above the glass transition temperature.
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