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Complete solvent removal required heating under vacuum up to well above the glass transition temperature.
We observed that the oil extraction rate decreases as the CO2 concentration in the solvent mixture increases, even in the region of complete solvent + oil miscibility.
In this work, volumes of up to 5 ml, at flow rates as high as 2 ml/min, were transferred from LC to GC with almost complete solvent removal even when working in reversed phase mode in the LC step.
Monitoring the amount of solvent eliminated as a function of the annealing parameters is important to design a proper treatment to ensure complete solvent elimination, crucial to obtain reproducible and stable material properties and therefore, device performance.
In fact, the bead formation prevention is attributed to the complete solvent evaporation at optimal distance.
Then, vinylated nanoparticles were dried at 110 °C until the complete solvent removal.
Similar(41)
Two sequences of potential measurements, one of increasing and the other of decreasing solvent content, are sufficient to obtain the pKa values of the acidic compound within the complete solvent-composition range in about 2 h.
The solution was allowed to stand for 2 hours for complete solvent-water separation.
After reaction was completed, solvent was removed using a rotary evaporator.
Once the previous simulations were completed, solvents containing CO2 were evaluated.
Once complete, the solvent was removed by lyophilisation.
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