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The lower organic phase was collected, vacuum evaporated, and the lipid extracts were subjected to FAME conversion (see below).
Under the direction of faculty member Mark Farfel, center staff collected vacuum sidewalk samples before, during, and after demolition took place in neighborhoods to measure lead content.
We collected vacuum cleaner dust if participants had used their vacuum in the past year and had owned half of their carpets for ≥5 years.
During the first round of dust sampling (2001 2007), we collected vacuum cleaner dust and administered a questionnaire during an in-home visit.
Resource-intense techniques such as active air sampling and field-technician collected vacuum dust have been used successfully in the past; however, these methods may be too costly for large-scale cohort studies.
On November 28, guided by findings from epidemiologic investigations at the Brentwood PDC, we collected vacuum and moist synthetic 2x2-inch surface wipe samples from all letter-canceling and -sorting machines (13 ).
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Supernatants were collected, vacuum-dried, re-dissolved in 0.5 µl 0.1% trifluoroacetic acid and added onto a matrix consisting of 0.5 µl of 5 mg/ml α-ciano-hydroxycynamic in water∶acetonitrile (2∶1) with 0.1% trifluoroacetic acid.
Supernatants were collected, vacuum-dried, and re-dissolved in 50% ACN and 0.1% trifluoroacetic acid (TFA) for MS analysis.
Substrate as well as product peaks were collected, vacuum-dried twice, and redissolved in order to remove deuterium incorporated into backbone amides.
Supernatants were collected, vacuum-dried and resuspended in 15 μl of pH 1.9 buffer (formic acid 2.3%, acetic acid 2.9% v/v).
The precipitate was collected by vacuum filtration and dried under vacuum to give macrocycle 4 as a black solid (282 mg, 198 μmol, 74%%).
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