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The polymer was collected filtration, washed with water, ethyl alcohol, water again and dried in a vacuum oven at 60°C for 24 h.
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Subsequently, the resulted solid was collected by filtration, and the filtrate was concentrated again and kept at 2 8°C for overnight.
The concentrated filtrate was sonicated in hexanes (20 mL/mmol) and the solid collected by filtration to give the product, which was purified by recrystallization from acetone.
The liquid was collected by filtration.
The formed precipitate is collected by filtration, washed with ethanol and crystallized from ethanol.
The solid product was collected by filtration to give the corresponding products 9a,b.
The precipitate was collected by filtration to afford the product as yellow crystals (90%).
Meanwhile, the powder of the suspension was also collected by filtration for characterizations.
The final product was collected by filtration and vacuum dried at 45°C for 2 days.
The final product was collected by filtration and dried at 45°C under vacuum.
Crude DFOD was collected by filtration and re-crystallized twice from methanol/water for purification.
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