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The clean-up procedure involved a SPE on C18 cartridge.
The amounts of solid sorbents for clean-up procedure were optimized by using experimental design.
Method optimization was predominantly focused on the simplification of extraction and clean-up procedure recommended by column producers.
A clean-up procedure was used for urine samples that consisted of a solid-phase extraction using C8 cartridges.
Without tedious clean-up procedure, analytes were extracted from the sample to the adsorbent and organic solvent and then desorbed in acetonitrile prior to chromatographic analysis.
The use of GCB for SPE allowed to obtain with a single clean-up procedure excellent recoveries ranging between 75 and 110% (relative standard deviation <16%).
Similar(26)
The extraction and clean-up procedures were carried out simultaneously in a single step.
The proposed irradiation techniques will eliminate the need for production shut down due to clean-up procedures.
These methods are restrictive for the quantification of salivary T, and require complicated clean-up procedures and expensive instruments.
The orientation maps were then subjected to a series of well-defined clean-up procedures for removal of badly indexed points and pseudosymmetry boundaries.
These methods are quite accurate, but they are dependent on multi-step sample clean-up procedures and are therefore relatively expensive and time consuming.
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