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Further, it is not clear that these two rules would remain robust as sample size increase, while, from Table 2, our heuristic rule for a seems much less affected by changes to sample size than is the case for r and k.
Although methods for valid changes to sample size parameters mid-trial are emerging, 37 no such method was mentioned in any study in our sample.
This methodology was adopted since it minimised the contamination of the sample from fixing and mounting agents, negated possible changes to sample biochemistry via conventional paraffinisation and deparaffinisation procedures, and allowed additional Raman spectral data to be collected without the background affects associated with glass substrates.
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Results indicate that ball milling of carbon nanotubes is a rather complex process and that it can cause several morphological changes to samples besides the well-known cutting effect.
Ofqual has asked all the exam boards to make the changes to their sample material and submit them for approval by the end of June.
Nevertheless, changes to the sample caused by irradiation are not only restricted to its organic ligands.
This is especially important when numerous acquisitions are required for a single data set, and time induced changes to the sample must be kept at a minimum.
The remainder of Table 3 shows the consequences of some changes to the sample necessitated by the aggregation of MSAs/PMSAs to MSAs/CMSAs, and of other changes to the data or specification.
Irradiation of homopolymeric Aβ16 22-BP20 aggregates for 60 min at 365 nm did not cause changes to the sample, and accordingly, nor did irradiation of aggregated Aβ16 22·Aβ16 22-BP20.
Four elements were not used, due to either very low concentrations in some samples (at detection limits: P, V, Cr, Rh) or possible changes due to sample preparation (Cl).
However, because of superimposition of dental structures or irreversible changes to tooth samples, the results obtained by these methods are not completely reliable (Song et al. 2010).
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