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The corrosion rate was evaluated by measuring the weight change of the samples and by cross-section examinations.
Macroscopically uniform deposition was achieved by exploiting the self-limiting nature of the reaction and the extent of deposition was monitored by the weight change of the samples.
This fact was accompanied by a physical change of the samples, fusion of microspheres to form large particles, which also fusion to form a unique mass of polymer; moment from that the degradation process was quicker.
This was achieved by designing an irradiation chamber and stage that allows for load application and removal, provides a method for controlling and monitoring temperature and proton flux, and a means to make in situ measurement of dimensional change of the samples during the experiment.
Figure 4a, b shows the density change of the samples with increasing the sintering temperature from 1300 to 1800 K.
Notably, such absorption enhancement in the visible region is also according to the color change of the samples as shown in the inset of Fig. 3a, b.
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The physical change of the sample was further analyzed with circular dichroism spectroscopy.
Adsorbed amount was monitored by the weight change of the sample.
The intensity, wavelength, and linewidth of the absorption peak were changed by the number of layers and resulted in a colour change of the sample if they were placed on a metal substrate.
A common approach to overcome this problem consists of an adaptive change of the sampling time according to reference/disturbance period variations.
For this purpose, a measuring device was developed that monitors the weight change of the sample with a resolution of 5 mg.
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