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Certification was performed using two different types of species-specific isotope-dilution mass spectrometric (SSID MS) method gas chromatography coupled with inductively coupled plasma mass spectrometry (SSID GC ICP MS) [ 4] and SSID GC MS combined with a microwave-assisted extraction in which a mixture of Sn-enriched butyltins synthesized in our laboratory was used as a spike.
Certification was performed by use of three different types of species-specific isotope-dilution mass spectrometry (SSID MS)—SSID GC ICP MS, SSID GC MS, and SSID LC ICP MS, with Sn-enriched organotin compounds synthesized from Sn-enriched metal used as a spike.
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Creating the requisite evidence for certification can be a challenging task due to the sheer size of the textual standards based on which certification is performed and the amenability of these standards to subjective interpretation.
The quality control aiming at certification is performed by an appropriate division of LANADA.
Certification procedure: During the initial phase from November 2001 to June 2003, test and pilot certifications were performed.
To study the problems faced during quality assurance and certification activities, a case study was performed on legacy software used for thermal analysis of a fuelpin in a nuclear reactor.
This was a religious ceremony that acted as the certification of the census, and was performed before the Century Assembly.
Analysis was performed under the certification of the ethics board of Tokushima University Hospital.
Determination of the organotin compounds in the candidate material by the six analytical methods was performed for the certification.
The physical examination was performed by an experienced physician with board certification in internal diseases and nephrology.
Transthoracic lung ultrasound was performed offline by an experienced investigator with level-3 certification [ 25], who was unaware of any other hemodynamic measures.
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