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Small cells arising from the cut-cell refinement are merged to improve the stability and performance.
Cell parameter refinement was performed by Celref version 3 software.
Also, cell parameter refinement was calculated by Celref software version 3.
Also, cell parameter refinement was calculated by Celref software version 3. SK got his B.S. degree from the University of Birjand in the field of applied chemistry in 2007.
Also, cell parameter refinement was reported by celref software version 3. In a typical synthetic experiment, 0.400 g (5.80 mmol) of LiNO3 (Mw = 68.95 gmol−1) and 0.522 g (8.69 mmol) of SiO2 (Mw = 60.08 gmol−1) were added to 60 mL of hot aqueous solutions of 0.3 M NaOH under magnetic stirring at 80 °C.
In order to obtain the cell length, Rietveld refinement was applied to fit the XRD data using Maud software [27].
The cell length after refinement was ca. 3.85 Å, lower than that of Pt and larger than that of Ni. Figure 3 shows the XPS spectra of the as-synthesized Pt3Ni microspheres.
The structure was obtained by rotating a rigid fragment in the unit cell in discrete steps; no refinement was attempted.
The unit cell does not change, the Rietveld refinement was hampered by preferred orientation and it appears that peak asymmetry was not modelled.
In the presence of adventitious moisture, the amorphous GeSx is oxidized to a crystalline phase identified by X-ray photoelectron spectroscopy, Raman spectroscopy and PXRD cell refinement to be hexagonal GeO2.
Therefore, a monophasic Rietveld refinement was applied for the LaSrAl0.6Cu0.4O4−δ sample by FULLPROF program, using reflections associated to tetragonal cell.
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