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Making a choice of laboratory scale reactor for kinetic studies or catalyst tests is not an easy task above all in case of three-phase reactions.
Our results also suggest that isothermal fixed bed catalyst tests cannot guarantee the best conversion and selectivity for complex ODH reactions.
Catalyst tests should be carried out both in fixed beds and micro fluidized beds with back mixing as early as in the stage of catalyst screening and development.
The catalyst tests employed a fixed bed reactor system, connected with gas chromatography system (online GC, off line GC/MS).
As far as the aged catalyst tests are concerned, it is worth mentioning that the lower SSA penalizes T10%, but T50% still remains within the range of the other fresh catalysts.
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The information from catalyst testing should be scalable.
Graduate student Jin Suntivich, lead author of the Nature Chemistry paper, holds up an electrochemical cell used for catalyst testing.
This enables parallel catalyst testing, which enhances the number of catalysts tested significantly and reduces the time for kinetic studies.
A differential packed-bed reactor microfabricated in silicon is presented for heterogeneous gas phase catalyst testing.
The paper presents the coupled results on reactor structure modelling and the catalyst testing.
The simulation results are compared with the Pt catalyst test results.
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