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The catalyst loading on CFP electrodes was 1 mg cm−2 for all materials.
If films with low catalyst loading are used, oxidative damage of the catalyst is observed (See Supplementary Fig. 6).
where jgeometrical is the geometric activity of the catalysts, and Mloading is the catalyst loading per geometric surface area.
While increasing the catalyst loading tends to decrease LAB yield.
Importantly, the high selectivity was maintained while lowering the catalyst loading to 1.5 mol% (Table 1, entry 4, 84% isolated yield).
A reduction of the catalyst loading to 5 mol% Ni(COD)2 afforded a lower yield of 3a (Supplementary Table 5).
The deposition time effect on the catalyst loading and the effect of the catalyst loading variation on the yield of CNF growth on carbon paper were investigated.
Both methods can be repeated to increase the catalyst loading.
High temperature (∼650 °C), and high catalyst loading (∼100%) are favorable for hydrogen production.
Five relevant factors were investigated: temperature, air pressure, catalyst loading, air flow rate and reaction time.
The investigated parameters include the membrane thickness, electrode compression ratio, electrode pretreatment and catalyst loading.
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