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Hydraulic press can be used to cast the samples at lower degree of saturation.
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The TEM specimens were prepared by drop casting the sample on the surface of the carbon coated copper grid.
The HRTEM specimens were prepared by drop casting the sample dispersion onto copper grid with holey carbon film and were dried under room temperature.
The HRTEM specimens were prepared by drop casting the sample dispersion onto a carbon-coated 300-mesh copper grid and were dried under room temperature.
Samples for Scanning Electron Microscopy (SEM) were prepared by drop casting the sample onto an aluminium stub and coated with platinum prior to imaging to minimize surface charging.
For X-ray photoemission spectroscopy (XPS), samples were prepared by drop casting the sample on a 100 nm evaporated thin film coated Au substrates, and measurements were carried out using Thermo K-Alpha XPS instrument at a pressure better than 1×10 9 Torr (1 Torr = 1.333×102 Pa).
Once cast, the test samples were first exposed to elevated temperatures ranging from 100 to 800 °C, and then allowed to cool down slowly to ambient room temperature of 20 °C before being tested to failure.
After casting, the brick samples were stored at 35 °C and a relative humidity of 50% until the ages required for testing.
In the case of solution cast samples the melt viscosity increases as the percentage of graft copolymer increases and the blend becomes more sensitive to temperature in the presence of graft copolymers.
Moreover, the representation of (1) allows us to re-cast the pure-color sampling structure in terms of sampling structures c α and c β associated with the difference channels x α and x β.
The solvent effect was annulated by casting the discs containing the samples (PCV, CHV, CHL and EPE) before placing them in the agar.
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