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The reaction was carefully heated until all the solids dissolved and a brown solution was obtained and then a solid product was formed, which was isolated by filtration.
2,4-Pentanedione (1.03 mL, 10 mmol) and powdery boric anhydride (0.52 g, 7.5 mmol) were mixed separately, carefully heated with stirring to obtain a paste, and added to the mixture of dimethoxybenzaldehyde and tributyl borate.
To compound 4 (0.01 mol) dissolved in 50 mL absolute ethanol was added slowly with shaking, ethoxymethylenemalononitrile (0.01 mol), after addition of about half of the quantity, the solution was carefully heated to boiling.
The plates were carefully heated at 100°C for optimal colour development.
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Take the heat gun and carefully heat up the blade until it is able to bend.
Use a lighter to, carefully, heat the entire edge of each circle.
Another way to warm the brandy is to carefully heat the glass over an open flame.
Using a torch, carefully heat the dried paint until it's soft enough to dig out with a safety pin.
Briefly, with the aid of a connector and a Hamilton syringe, a small volume of Vit 2 is aspirated followed by the embryos in Vit 2 then another small volume of Vit 2. The lower end was carefully heat sealed and the cover sleeve was slid down.
But at her house, in Williamstown, Mass., the ingredients are all mixed in order, very carefully, and heated to a bare simmer.
You may be able to use it again if you carefully re-heat it.
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