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To study the effect of calcination time, the samples were calcined for 1, 2, 3, 4 and 5 h at 300 °C.
When alumina particles calcined at the desired temperature in order to obtain certain crystal types, the calcination time depends on the size of the precursor.
The mean strength increases as calcination time increases.
The calcination time ranged from 1 h to 7 h.
When the calcination time exceeds 5 h, surface cracks were observed as shown in Fig. 1c for ones obtained at a calcination time of 7 h.
A longer material calcination time improves the deposition of internal features.
The intensity of the diffraction peaks increases and the peak widths decrease with the calcination time.
% of Ce loading, calcination temperature of 486 °C and calcination time of 4 h.
However, calcination time has no significant effect on Weibull's modulus in the experimental domain examined.
For the nanowires obtained at a calcination time ≤5 h, the surfaces are smooth as shown in Fig. 1b for ones obtained at the calcination time of 5 h.
The regeneration conditions including calcination temperature and calcination time were optimized.
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