Exact(3)
Among these are silica, obtained by calcination (heating) of silica gel; high-purity alumina, prepared by the calcining of specially prepared aluminum hydroxide; and silica-alumina mixtures.
To determine the best conditions for obtaining (CoAl2O4) in this study, five factors were chosen as input variables at levels determined for this study: citric acid concentration (stoichiometric), pyrolysis time (h), temperature (°C), calcination heating time and rate (°C/min).
The study of the quantitative influence of some OMA synthesis conditions (water aluminium ratio (H2O: Al), ageing temperature (Tag), and calcination heating rate (rcal)) on the resulting OMA textural properties (specific surface area (SBET), pore volume (Vp) and average pore diameter (APD)) was carried out using a Box-Wilson Central Composite Design Face Centred (CCF, α: ±1).
Similar(57)
The matrix film provides a surface platform to spatially segregate small volumes of reagents, which is efficiently removed by calcination during heating steps.
The zeolite dispersion in the sepiolite matrix may prevent structural damage during calcination, as heat can dissipate more effectively and organic residues may be more easily removed.
The calcination temperature, the heating rate, the moisture content and the calcination time respectively, all have strong effects on the resulting strength of the catalyst.
A new concept with an indirectly heated calciner is presented, where the heat for calcination is transferred by means of heat pipes from an external combustor.
Specifically, these look at varying the standard calcination techniques using heat treatments in He (rather than calcination in air) and lower temperature calcinations (200 °C rather than 500 °C).
These microstructures resulted from different processing parameters such as heating rate, calcination temperature and post calcination annealing, and made it possible to study the influence of the electrode microstructure on the electrochemical performance.
Samples were also synthesized using conventional calcination methods (applying slow heating and long exposure times, SHLE series).
The results of the synthesis method is to produce high shear and in situ calcination by shock wave heating and high Reynolds numbers.
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