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Furthermore, the precursor stoichiometry and cooling rate as well as the calcination atmosphere and crystallization time turned out to interact.
The calcination atmosphere turned out to be the most important to avoid the formation of the Sillenite secondary phase, Bi12TiO20.
The electrochemical performance depended on the Ti content and calcination atmosphere.
The influence of the calcination atmosphere on the Nb-doped ceria has also been studied.
The relative order of importance of the factors evaluated was found to be support > pretreatment > loading > calcination atmosphere > calcination temperature > precursor salt.
By means of a series of physicochemical and electrochemical characterizations, different calcination atmosphere show great effect on the properties of the resulting materials.
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The effects of calcination atmospheres (O2 and N2) and the preparation methods (impregnation and electroless deposition) on the physiochemical and catalytic properties of Pd/TiO2 catalysts were investigated in the selective hydrogenation of acetylene.
The Mo-V oxide catalysts were prepared by a simple hydrothermal method under different synthesis and calcination atmospheres and were characterized by in situ XRD, TPD-NH3, N2 adsorption/desorption, X-ray absorption near vanadium K-edge spectroscopy and thermogravimetry.
The obtained precursors were transformed into the mono-phase oxide forms by calcination in air atmosphere.
The submicron size zeolite-Y particles were grown with entrapment of the GO nanosheets and the complete removal of PDDA-GO by calcination under air atmosphere assisted nanoporosity generation in the zeolite crystals.
The exactly defined temperature schedules of calcinations and atmosphere were suggested according to the results obtained from TG/DSC analysis.
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