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The extent of completion was monitored by the square wave stripping voltammetry.
The reaction is in a continuous phase and controlled by the square wave with different duty cycles: (a) 50%, (b) 75%, (c) 100%.
The detection mechanism was based on the monitoring of the electrochemical current response change of TB by the square wave voltammetry (SWV) when immunoreaction occurred on the surface of electrode.
Determination of IMD by the square wave stripping voltammetry method represented a wide linear range of 0.059 0.791 μg L−1 with a detection limit of 0.0125 μg L−1.
The signals were determined by the square wave voltammograms and were linear with the concentration of lysozyme in the range from 7 nM to 30 nM, with a detection limit of 0.45 nM.
The electrochemical current intensity for the cathodic reduction of AC recorded by the square wave voltammetric technique was nearly 10 times higher than that generated by the differential pulse excitation mode.
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The stability was followed by the variation on polaronic (500 nm) and bipolaronic (800 nm) absorption along treatments by the square waves of potential between zero and − 800 mV.
The binding is monitored by following the change in the square wave voltammetry (SWV) reduction peak signal of ferrocyanide/ferricyanide redox couple due to the removal of the negatively charged aptamers from the surface upon protein binding.
In this method, the frequency of the sinusoid wave is held constant, and particles can be selected based on size by changing the frequency of the square wave using a simple electrode design [ 106].
The square wave output produced by the inverter is fed to a low pass filter to obtain a sinusoidal wave.
In this work, platinum nanocrystals of different shapes, octahedra with low-index facets, tetrahexahedra and concave hexoctahedron enclosed with high-index facets, were synthesized by the square-wave-potential method (SWP).
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